Jurnal Ilmiah Ibnu Sina, 9. Oktober 2024, 457-467 p-ISSN: 2502-647X. e-ISSN: 2503-1902 THE IMPACT OF PVA CONCENTRATION ON THE PHYSICAL QUALITY OF THE Eleutherine palmifolia (L. ) Merr LEAVES PEEL-OFF GEL MASK Eka Kumalasari*. Erna Prihandiwati. Muhammad MaAoruf. Novia Ariani. Senya Puteri Amelia. Muhammad Hafizh Abiyyu Fathin Fawwazi Sekolah Tinggi Ilmu Kesehatan ISFI Banjarmasin *Email: ekakumalasari260989@gmail. Artikel diterima: 01 Oktober 2024. Disetujui: 29 Oktober 2024 DOI: https://doi. org/10. 36387/jiis. ABSTRAK Bawang dayak (Eleutherine palifolia Merr. ) merupakan obat tradisional yang digunakan oleh masyarakat daerah Kalimantan Tengah untuk mengobati berbagai Daun bawang dayak mengandung senyawa flavonoid. Ekstrak daun bawang dayak memiliki aktivitas antioksidan yang sangat kuat dengan nilai IC 50 45,33 ppm. Antioksidan efektif untuk mencegah kerusakan kulit akibat paparan sinar ultraviolet. Potensi daun bawang dayak sebagai antioksidan dapat dimanfaatkan dalam bentuk masker gel peel-off. Masker gel peel-off diformulasikan dengan variasi basis polivinil alkohol (PVA) F1 10%. F2 12%, dan F3 14%. Konsentrasi PVA merupakan faktor terpenting yang berpengaruh terhadap kinerja pembentukan film dalam masker gel peel-off. Penelitian ini bertujuan untuk mengetahui pengaruh variasi konsentrasi PVA terhadap sifat fisik dan aktivitas antioksidan masker gel peel-off daun bawang dayak. Seluruh formula dilakukan uji organoleptis, homogenitas, daya sebar, nilai pH dan kecepatan pengeringan serta aktivitas antioksidan yang diuji menggunakan metode DPPH. Hasil pengujian menunjukkan seluruh formula masker gel peel-off memenuhi persyaratan uji sifat fisik dan memiliki aktivitas antioksidan. Berdasarkan analisis statistik menggunakan one way anova variasi konsentrasi PVA memberikan pengaruh yang signifikan . <0,. pada kecepatan pengeringan masker peel-off. Kata kunci: Bawang dayak. Antioksidan. Masker. PVA ABSTRACT The natives of Central Kalimantan utilize Eleutherine palmifolia . ) Merr as a traditional medicine to treat various diseases. Eleutherine palmifolia leaves are rich in flavonoid substances. Eleutherine palmifolia leaves extract has an IC50 value of 45. 33 ppm, indicating significant antioxidant activity. Antioxidants are helpful in reducing the risk of UV radiation-induced skin damage. Eleutherine palmifolia leaves have antioxidant properties that can be used as a peel-off gel Polyvinyl alcohol (PVA) bases come in various formulations for peel-off gel mask that F1 10%. F2 12%, and F3 14%. The concentration of PVA is the most significant element affecting how well peel-off gel masks create films. This study aims to determine the impact of PVA concentration on the physical of the Eka Kumalasari, dkk | 457 Jurnal Ilmiah Ibnu Sina, 9. Oktober 2024, 457-467 p-ISSN: 2502-647X. e-ISSN: 2503-1902 Eleutherine palmifolia leaves Peel-off gel mask. All formulas are tested for organoleptics, homogeneity, spreadability, pH value, and drying speed. The results showed that all peel-off gel mask compositions pass the physical properties test. one-way ANOVA statistical analysis reveals a significant variation in the preparations drying speeds . <0,. Keywords: Eleutherine palmifolia ,Antioxidant. Mask. PVA. INTRODUCTION One popular plant in Kalimantan antioxidant properties that can be used in traditional medicine is the used as a peel-off gel mask. Peel-off Eleutherine (L) Merr gel mask preparations are one of the leaves (Novaryatiin et al. , 2. most well-liked cosmetics due to their simplicity of usage. The mask is Eleutherine easier to use once it dries because the gel layer can be removed from the conditions like blisters, but the skin without having to be rinsed with community rarely uses the leaves water (Andini et al. , 2. Polyvinyl (Siswanto Syamsul et al. , 2. alcohol (PVA) is the base for peel-off Eleutherine palmifolia leaves are rich Because PVA has sticky in alkaloids, flavonoids, saponins, qualities, it can form a film layer that steroids, and triterpenoids (Idrus et is effortlessly peeled off after drying7, , 2. With an IC50 value of contributing to the peel-off effect. 33 ppm. Eleutherine palmifolia The primary factor influencing peel- leaves extract is reported to have off mask film formation performance is PVA concentration. As a result, it is (Kumalasari & Prihandiwati, 2. necessary to adjust the PVA content Antioxidants help mitigate the effects and test the mask physically, ensuring of aging and ultraviolet (UV) light- induced skin damage. Antioxidants can reduce free radicals, lowering the value, and drying speed tests. Dayak Eleutherine palmifolia leaves have likelihood of oxidation reactions (Priani et al. , 2. Eka Kumalasari, dkk | 458 Jurnal Ilmiah Ibnu Sina, 9. Oktober 2024, 457-467 p-ISSN: 2502-647X. e-ISSN: 2503-1902 Extract weight METHODS %Yield = Simplicia weight ycu100 The equipment used was a rotary (Ohaus. , glassware, water bath (Mamer. , universal pH (Merc. The materials used in this research were Eleutherine PVA. HPMC, propylene glycol. using aquadest, taken as much as 1 ml, is inserted into the reaction tube, then added Pb acetate . When the extract causes the yellow color of the encapsulation, the positive extract Making Peel-Off Gel Mask Making Extract Formulation Eleutherine palmifolia leaves are obtained from the Petuk Katimpun Extract that has been dissolved Preparation of samples Phytochemical screening Palangkaraya. Table 1. Eleutherine palmifolia leaves peel-off gel mask formulation Central Concentration (%) FII Fi Function Eleutherine palmifolia leaves PVA Active Film layer temperature of 50 C. The results of HPMC drying are pulverized into a powder Humectant Methyl paraben 0,02 0,02 0,02 Preservative Propyl paraben 0,05 0,05 0,05 Preservative Lily oil Corigen odoris Aquadest ad Solvent Kalimantan. After being cleaned by running water, the leaves are chopped and then dried in the oven at a 5 liters of 70% ethanol were macerated with 500 g of constantly stirred. A thick extract is produced by filtering and evaporating the macerate. Organoleptic extract testing is carried out using the five senses by describing color, smell and consistency as simply and objectively as possible. The extract obtained was Materials Gelling agent After adding hot distilled water to the evaporator cup, stirring until the PVA fully expands. Additionally. HPMC was generated by expanding the material to its ideal size using hot distilled water. PVA and HPMC are combined and then ground into a calculated by the yield Eka Kumalasari, dkk | 459 Jurnal Ilmiah Ibnu Sina, 9. Oktober 2024, 457-467 p-ISSN: 2502-647X. e-ISSN: 2503-1902 consistent powder. After adding the 100-gram weights, and give it one dissolved propyl paraben, methyl minute to settle. When the stock stops spreading, the spreading diameter is then measured at each progressive thoroughly mixed. Next, gradually Spreadability at 5 to 7 cm Eleutherine reveals a semi-solid consistency that palmifolia leaves extract in 70% is extremely pleasant to work with. ethanol and mill everything until it is pH Test When For testing pH, one gram of the mixture is consistent with 100 g, add the Lili fragrance and the remaining distilled water is added, the pH paper crushed distilled water. is dipped into the preparation, and the Peel-Off Gel Mask Evaluation results are adjusted to the pH number Organoleptic test by waiting. For a stable reading, the Organoleptic pH of the gel should be between 4. 5, which is the same as the pH considering the mask's color, odor, of the skin. and shape. It is also simple to apply Drying speed Test and does not include any rough The test for dry time was conducted by evenly applying 0. Homogeneity Test gram of gel to an area of 2. 5 x 2. 5 cm An excellent gel dosage form on the arm and then timing the doesn't include rough granules or amount of time needed for the To conduct this test, the gel preparation to dry, which is the preparation is applied to two glass amount of time from the application of the gel mask until the formation of Spreadability Test a dry and elastic layer. Remove the To determine its spreadability, place one gram of mask on a glass skin's surface without leaving a gel mass behind. scale, top it off with the same glass, increase the load with 50-gram and Eka Kumalasari, dkk | 460 Jurnal Ilmiah Ibnu Sina, 9. Oktober 2024, 457-467 p-ISSN: 2502-647X. e-ISSN: 2503-1902 Data Analizes It is shown by the color of the Data analysis was carried out SPSS Varying PVA concentrations are Statistics software. Organoleptic and used to make peel-off gel mask Polyvinyl alcohol is used in carried out descriptively. Meanwhile, the formulation of peel-off gel masks analysis of pH, spreadability, drying as an agent that creates an elastic film speed was carried out using SPSS layer that allows the formula to be The analysis carried out was peeled off. HMPC is a gelling normality and homogeneity tests. ingredient that improves the peel-off mask base's viscosity. Propylene treatment groups, a one-way analysis glycol, a humectant that can stop of variance (ANOVA) was carried out excessive water evaporation in the gel if the data was normally distributed preparation during storage and during and homogeneous. If the data is not skin application, is added to the normally distributed, a preparation in an attempt to preserve yellow depot. Kruskal- Wallis analysis is performed. its stability (Samsul et al. , 2. In addition, propylene glycol has RESULTS AND DISCUSSION the ability to raise the preparation's The 64. 8-gram extract had a thick viscosity, making it thick enough to consistency, a brown color, and a rub on face skin easily while strong fragrance. In this investigation, maintaining flow. In addition, rising the extract yield value was 12. humidity will have an impact on the The extract was discovered to contain properties of the polyvinyl alcohol flavonoid compounds in the findings The rise of moisture content of the phytochemical screening test. will render the layer softer and more The positive result is characterized by flexible, which will enhance the layer's properties. Since humectants composite to be oxidized by a Pb2 are hygroscopic and typically exist in metal by forming a complex with lead liquid form, they may have an impact Eka Kumalasari, dkk | 461 Jurnal Ilmiah Ibnu Sina, 9. Oktober 2024, 457-467 p-ISSN: 2502-647X. e-ISSN: 2503-1902 on the gel preparation's physical characteristics (Sari et al. , 2. A peel-off mask's perfect qualities would be to be free of abrasive Methylparaben and propylparaben particles, non-toxic, irritant-causing, are two of the preservatives applied to and able to cleanse the skin. Capable the base preparations to stop germs of moisturizing the skin, creating a and fungi from growing. Because consistent thin layer level, tightening they can intensify their effect on the skin, and drying in five to thirty certain bacteria and fungi, these two Peel-off masks must to be substances are utilized in tandem. simple to apply and painless(Grace et Distilled water is utilized as a solvent , 2. (Sari et al. , 2. Figure 1. Eleutherine palmifolia leaves gel peel-off mask Table 2. Evaluation results of the physical properties of the peel gel mask of Eleutherine palmifolia leaves extract Formulation Parameter i Chocolate, lily Chocolate, lily Chocolate, lily Organoleptis aroma, thick aroma, thick aroma, thick Homogenitas Homogen Homogen Homogen Spreading Power 5-100 g 3,8 - 6,5 3,9 - 6,7 3,2 - 6,4 Drying Time 19,67 A 0,58 19,00 A 0,58 16,67 A 1,00 (Minut. The color, odor, and consistency of Because it has to do with the Eleutherine palmifolia leaves how well the product is received by extract gel peel-off mask were consumers, this test is carried out. Organoleptic examinations indicate Eka Kumalasari, dkk | 462 Jurnal Ilmiah Ibnu Sina, 9. Oktober 2024, 457-467 p-ISSN: 2502-647X. e-ISSN: 2503-1902 that the peel-off gel mask preparation recipe has a thick viscosity, lily irritated (Khaeri Nursamsiar. It is evident from the tests that every peel-off gel mask recipe The purpose of the homogeneity satisfies the required pH value. The test is to verify that the active Spreadability test results data were analyzed using one way anova and ingredients are all combined evenly obtained a significance value of (Wulandari & Wahyudi, 2. The >0. 05, which means there was no absence of rough, lumpy granules and influence between variations in the the uniform distribution of color in PVA on the pH of the the peel-off gel the mask preparation are signs of The steps involved in PVA HPMC The results of testing the mask preparation's spreadability indicate combining them are crucial markers that it is simple to apply to the skin, in the creation of consistent mask making it comfortable to wear (Anindhita et al. , 2. It will be producing a uniformly dispersed simpler to apply the mask preparation mask color is to dissolve the extract in to the skin's surface due to its high ethanol before adding it to the mask spreading capacity. Testing reveals that every peel-off gel mask formula Another This pH measurement seeks to satisfies the 5-7 cm spreadability demonstrate the pH range of 4. 5 to 6. criteria (Amaliah et al. , 2. The that the mask ought to possess to be spreadability test results data were able to function well when applied to analyzed using one way anova and the skin (Rahim & Nofiandi, 2. obtained a significance value of When the preparation is basic, it will >0. 05, namely 0,835, which means result in smooth core skin, quickly there was no influence between dry, and affect the elasticity of the variations in the concentration of skin, whereas if the formulation is PVA on the spreadability of the peel- acidic with a pH below the pH range. The Eka Kumalasari, dkk | 463 Jurnal Ilmiah Ibnu Sina, 9. Oktober 2024, 457-467 p-ISSN: 2502-647X. e-ISSN: 2503-1902 spreadability test findings indicate some of the variables that might affect that the spreadability value declines drying time (Kartikasari & Anggraini, with increasing PVA concentration. All of the formulations satisfy the drying time specifications, according correlation with preparation viscosity: to the drying time test findings. It is the higher the viscosity of the preparation, the less spreadable it is preparation if it dries rapidly, as the on the skin. This is consistent with the application takes a short time to have an effect (Ayuchecaria et al. , 2. viscosity and particle diameter, as As may be shown, formula i has the stated by Stoke's law: the more quickest drying time, with a PVA significant the viscosity, the smaller content of 14%. The Drying speed test the particle diameter. results data were analyzed using one To figure out how long the preparation may dry after being significance value of <0. 05, namely applied to the skin, its drying time is 0,006, which means there Ideally, a peel-off mask influence between variations in the should dry in 15 to 30 minutes. One concentration of PVA on the Drying of the most crucial tests to do when speed of the peel-off gel mask This is due to the fact that peel-off preparations is the drying speed test. PVA which establishes how well the preparation responds to longer drying the more PVA value-added, the The peel-off gel mask is faster a preparation dries (Kartikasari a preparation for a mask that dries on & Anggraini, 2. The chemicals the skin, solidifies, and leaves behind that go into a peel-off gel mask determine its physical properties. The thickness of PVA is a film former that can be used application, the temperature, and the at concentrations ranging from 10- air during the application process are Eka Kumalasari, dkk | 464 Jurnal Ilmiah Ibnu Sina, 9. Oktober 2024, 457-467 p-ISSN: 2502-647X. e-ISSN: 2503-1902 16% for peel-off gel face masks (Noviana Suhery et al. , 2. CONCLUSION The results showed that all peel-off gel mask compositions pass the physical properties test and have one-way ANOVA statistical analysis reveals a preparations drying speeds . <0,. REFERENCES